Zinc in PDB 3rto: Acoustically Mounted Porcine Insulin Microcrystals Yield An X-Ray Sad Structure

The structure of Acoustically Mounted Porcine Insulin Microcrystals Yield An X-Ray Sad Structure, PDB code: 3rto was solved by A.S.Soares, M.A.Engel, R.Stearns, S.Datwani, J.Olechno, R.Ellson, J.M.Skinner, M.Allaire, A.M.Orville, with X-Ray Crystallography technique. A brief refinement statistics is given in the table below:

Resolution Low / High (Å)	40.85 / 1.80
Space group	H 3
Cell size a, b, c (Å), α, β, γ (°)	81.700, 81.700, 33.800, 90.00, 90.00, 120.00
R / Rfree (%)	18.1 / 22.3

The binding sites of Zinc atom in the Acoustically Mounted Porcine Insulin Microcrystals Yield An X-Ray Sad Structure (pdb code 3rto). This binding sites where shown within 5.0 Angstroms radius around Zinc atom.
In total 2 binding sites of Zinc where determined in the Acoustically Mounted Porcine Insulin Microcrystals Yield An X-Ray Sad Structure, PDB code: 3rto:
Jump to Zinc binding site number: 1; 2;

Zinc binding site 1 out of 2 in the Acoustically Mounted Porcine Insulin Microcrystals Yield An X-Ray Sad Structure


Mono view


Stereo pair view

A full contact list of Zinc with other atoms in the Zn binding site number 1 of Acoustically Mounted Porcine Insulin Microcrystals Yield An X-Ray Sad Structure within 5.0Å range: probe atom residue distance (Å) B Occ B:Zn31 b:28.4 occ:0.31 NE2 B:HIS10 2.1 23.4 1.0 O B:HOH36 2.7 35.3 1.0 CD2 B:HIS10 3.1 21.9 1.0 CE1 B:HIS10 3.1 27.2 1.0 O B:HOH32 3.6 76.1 0.3 ND1 B:HIS10 4.2 27.9 1.0 CG B:HIS10 4.2 24.4 1.0 O B:HOH34 4.5 56.4 0.2

Zinc binding site 2 out of 2 in the Acoustically Mounted Porcine Insulin Microcrystals Yield An X-Ray Sad Structure


Mono view


Stereo pair view

A full contact list of Zinc with other atoms in the Zn binding site number 2 of Acoustically Mounted Porcine Insulin Microcrystals Yield An X-Ray Sad Structure within 5.0Å range: probe atom residue distance (Å) B Occ D:Zn31 b:29.5 occ:0.30 NE2 D:HIS10 2.1 26.8 1.0 O D:HOH32 2.4 46.0 1.0 CE1 D:HIS10 3.0 27.4 1.0 CD2 D:HIS10 3.1 25.1 1.0 O D:HOH36 3.8 91.7 0.3 ND1 D:HIS10 4.1 26.2 1.0 CG D:HIS10 4.2 26.0 1.0 O B:HOH33 4.5 26.9 0.1 O D:HOH44 4.6 56.3 1.0 O D:HOH47 4.8 39.4 1.0

A.S.Soares, M.A.Engel, R.Stearns, S.Datwani, J.Olechno, R.Ellson, J.M.Skinner, M.Allaire, A.M.Orville. Acoustically Mounted Microcrystals Yield High-Resolution X-Ray Structures. Biochemistry V. 50 4399 2011.
ISSN: ISSN 0006-2960
PubMed: 21542590
DOI: 10.1021/BI200549X